ｻﾝﾌﾟﾙ: '191024 Sample ﾌｧｲﾙ名: 191024　10μg PB2.FD3 分析日時: '10:18:15, 10/24/2019 ｵﾍﾟﾚｰﾀ: 筑波大学 ｺﾒﾝﾄ: ' 光度計 ﾓﾃﾞﾙ: F-7000形分光蛍光光度計 ｼﾘｱﾙ No.: 2357-015 ROM Ver.: 5J14000 06 装置条件 測定ﾓｰﾄﾞ: 3次元 ﾃﾞｰﾀﾓｰﾄﾞ: 蛍光 励起開始波長: 200.0 nm 励起終了波長: 500.0 nm 励起側ｻﾝﾌﾟﾘﾝｸﾞ間隔: 10.0 nm 蛍光開始波長: 200.0 nm 蛍光終了波長: 700.0 nm 蛍光側ｻﾝﾌﾟﾘﾝｸﾞ間隔: 10.0 nm ｽｷｬﾝｽﾋﾟｰﾄﾞ: 30000 nm/min 励起側ｽﾘｯﾄ: 5.0 nm 蛍光側ｽﾘｯﾄ: 5.0 nm ﾎﾄﾏﾙ電圧: 700 V ﾚｽﾎﾟﾝｽ: 自動 ｽﾍﾟｸﾄﾙ補正: On ｼｬｯﾀ制御: On 等高線間隔: 50.000 装置関数 励起側(200〜500nm) ｽﾘｯﾄ：5.0/20.0nm ﾎﾄﾏﾙ電圧：400V 蛍光側(200〜500nm) ｽﾘｯﾄ：5.0/20.0nm ﾎﾄﾏﾙ電圧：250V 蛍光側(500〜900nm) ｽﾘｯﾄ：---/5.0nm ﾎﾄﾏﾙ電圧：400V 励起側(500〜900nm) ｽﾘｯﾄ：5.0/5.0nm ﾎﾄﾏﾙ電圧：350V ﾃﾞｰﾀﾘｽﾄ 200.000 210.000 220.000 230.000 240.000 250.000 260.000 270.000 280.000 290.000 300.000 310.000 320.000 330.000 340.000 350.000 360.000 370.000 380.000 390.000 400.000 410.000 420.000 430.000 440.000 450.000 460.000 470.000 480.000 490.000 500.000 200.0 9999.9 4140 26.52 9.449 18.63 13.59 12.14 15.62 13.38 13.89 12.71 11.35 10.97 8.916 9.164 7.845 7.997 7.358 6.938 6.450 33.11 39.98 6.036 4.482 3.946 3.162 2.707 3.166 2.979 2.541 2.122 210.0 539.3 9999.9 2636 22.83 13.92 10.24 9.875 8.051 8.710 8.842 8.783 7.192 7.019 6.572 5.456 5.061 4.692 4.546 4.201 3.627 4.516 6.756 40.62 42.04 3.518 2.335 2.219 1.690 1.568 1.691 1.926 220.0 97.65 545.0 9999.9 2315 20.94 12.59 9.957 8.491 7.649 6.203 6.366 5.431 5.049 4.691 3.975 3.291 3.371 3.419 2.895 2.383 2.008 2.044 3.281 7.235 54.45 50.68 2.716 1.471 0.959 1.059 1.032 230.0 61.50 103.1 584.6 9999.9 2637 18.99 11.02 9.258 7.576 6.500 5.330 4.495 4.179 3.611 3.385 2.952 2.673 2.535 2.303 2.192 2.048 1.775 1.540 1.608 3.221 10.78 100.1 75.08 3.258 1.075 1.063 240.0 77.41 93.60 138.9 626.7 9999.9 3274 21.01 12.34 8.083 6.527 5.915 5.057 4.172 3.408 3.401 3.059 2.580 2.150 2.285 2.055 1.837 1.560 1.420 1.265 1.559 1.668 4.887 19.93 206.8 157.6 4.980 250.0 154.2 128.1 94.38 148.9 662.7 9999.9 3885 21.57 13.40 8.520 6.372 5.423 4.377 4.041 3.758 3.115 2.729 2.582 2.301 1.918 1.545 1.537 1.465 1.255 1.290 1.370 1.393 1.856 9.043 43.28 399.6 260.0 254.2 159.1 117.1 83.08 160.6 724.6 9999.9 4034 27.49 15.55 9.376 7.278 5.143 4.458 3.586 3.393 2.897 2.858 2.465 2.194 2.041 1.847 1.629 1.692 1.421 1.286 1.201 0.985 1.808 2.895 16.42 270.0 388.1 236.5 141.3 68.40 69.74 145.1 695.5 9999.9 4259 31.01 16.42 10.69 6.988 5.645 4.498 3.780 3.248 3.184 2.820 2.574 2.036 1.984 1.901 1.754 1.552 1.484 1.269 1.081 1.303 1.550 2.453 280.0 482.5 320.0 213.4 109.1 72.83 74.39 127.6 750.1 9999.9 3864 33.46 17.62 10.82 7.289 5.806 5.331 4.259 4.167 3.478 3.401 2.737 2.148 2.014 2.120 1.797 1.796 1.797 1.547 1.612 1.763 1.486 290.0 1334 1421 1227 923.4 472.5 153.3 247.3 484.7 1187 9999.9 3831 37.85 18.80 12.68 8.494 6.825 5.296 4.565 4.514 4.160 4.023 3.276 3.116 3.385 3.312 3.107 3.435 3.048 3.448 2.937 2.288 300.0 3374 3599 3253 2678 1345 438.5 627.3 1338 1588 1307 9999.9 3598 41.23 22.01 14.01 9.095 7.273 6.069 5.605 5.401 5.294 5.470 5.177 5.780 5.878 6.367 7.649 6.908 7.182 5.000 4.432 310.0 4825 5206 4784 3905 2021 620.7 881.7 1849 2349 804.3 881.6 9999.9 3511 45.38 23.74 15.35 10.01 8.582 7.466 6.607 6.946 7.013 7.567 7.152 7.899 9.207 10.41 9.683 9.525 6.231 5.512 320.0 4548 5320 4813 4036 2074 615.9 886.9 1857 2303 859.7 145.4 862.2 9999.9 3688 47.07 25.10 16.42 11.19 8.896 7.875 8.004 8.109 7.655 8.284 8.871 9.302 11.01 10.13 9.990 6.884 5.831 330.0 4103 4489 4098 3380 1722 537.5 736.9 1503 1846 669.9 154.3 106.0 765.8 9999.9 3557 48.08 26.18 17.30 11.91 9.134 8.354 8.263 7.620 8.276 8.241 8.591 9.869 8.838 8.882 6.468 5.508 340.0 3355 3409 3211 2607 1419 484.7 590.6 1116 1369 552.6 121.9 102.6 111.3 695.5 9999.9 3569 48.47 26.11 16.63 12.13 9.863 8.495 7.899 8.211 8.119 8.258 8.951 7.851 8.145 6.339 5.317 350.0 2630 2513 2314 1921 1117 454.7 472.9 778.8 960.7 434.6 105.0 112.6 89.35 108.3 683.3 9999.9 3626 48.59 25.22 16.42 11.61 9.542 7.988 8.068 7.669 7.988 7.815 6.854 7.135 5.447 5.452 360.0 2202 2028 1597 1435 853.8 395.8 378.1 528.6 644.6 329.3 95.25 76.70 122.5 78.68 95.73 632.9 9999.9 3653 46.80 24.57 16.27 12.41 9.029 8.273 7.455 6.847 7.131 6.782 6.437 5.326 4.668 370.0 1906 1517 1262 1021 633.3 322.1 294.6 375.9 429.1 233.9 86.83 75.64 79.22 114.6 64.36 83.35 597.3 9999.9 3582 45.15 23.92 16.17 11.89 9.487 8.221 7.231 6.549 5.801 5.932 5.133 4.981 380.0 1577 1255 912.6 725.3 490.9 269.7 219.5 259.8 287.0 171.9 76.32 65.74 68.56 70.83 80.94 46.42 72.91 586.1 9999.9 3573 44.31 23.77 15.37 11.44 8.307 7.567 6.730 5.507 5.589 5.561 5.083 390.0 7754 970.3 724.9 536.1 391.6 228.4 170.3 195.2 204.2 125.7 65.86 60.32 62.64 59.39 64.73 59.47 45.38 76.65 584.7 9999.9 3765 44.64 23.14 16.23 10.46 8.274 7.175 5.600 5.621 5.322 4.985 400.0 9999.9 867.2 555.4 420.3 304.8 221.3 142.1 149.5 150.1 96.64 59.39 56.59 54.56 52.05 49.18 63.18 45.94 45.79 77.83 580.6 9999.9 3800 43.02 21.43 14.37 10.15 7.890 6.605 5.795 5.365 4.852 410.0 2639 9999.9 482.4 348.1 247.0 192.8 121.1 119.2 115.9 73.86 52.36 48.64 50.37 45.17 43.29 42.54 60.28 40.57 44.52 70.37 553.4 9999.9 3989 41.19 20.90 13.99 9.138 7.660 5.864 5.347 5.296 420.0 995.4 9999.9 438.1 289.8 215.2 184.5 108.5 97.10 88.17 63.69 44.89 43.44 43.26 41.39 38.88 37.38 38.49 53.29 38.11 37.85 58.27 542.7 9999.9 3895 38.75 19.36 12.88 8.843 7.723 6.342 6.140 430.0 856.4 4108 9999.9 251.3 207.0 166.8 93.73 79.39 74.18 52.03 40.01 40.83 37.67 37.66 35.96 35.11 31.82 35.91 39.14 28.00 26.89 54.27 530.3 9999.9 3738 39.19 18.94 11.73 9.068 6.745 6.442 440.0 799.7 723.4 9999.9 231.3 172.8 171.0 92.14 68.70 63.11 47.36 37.83 35.20 35.15 33.41 34.78 34.31 31.76 29.19 36.76 27.97 22.56 24.92 52.58 553.8 9999.9 3542 36.53 17.47 12.92 8.273 7.747 450.0 829.0 647.5 5000 9999.9 167.2 168.3 85.39 61.89 58.16 44.45 36.94 33.64 32.37 30.99 33.54 34.54 32.31 26.71 26.16 34.34 21.99 22.30 24.71 54.01 552.6 9999.9 3420 35.70 18.53 12.09 9.572 460.0 839.8 578.0 522.8 9999.9 192.4 179.0 83.81 60.25 53.91 42.50 33.43 31.52 30.61 28.68 31.84 34.25 29.29 25.88 25.09 23.30 29.50 20.25 21.47 26.01 52.75 526.3 9999.9 3574 35.98 17.94 13.51 470.0 938.4 643.6 408.9 5592 9999.9 173.1 94.05 58.40 49.83 43.40 34.11 31.35 31.37 29.33 31.70 32.66 30.43 24.44 22.74 21.05 22.75 26.50 24.37 26.33 27.45 51.64 538.3 9999.9 4164 37.70 20.26 480.0 829.8 542.0 307.4 411.7 9999.9 212.2 92.32 51.42 45.00 37.91 32.85 29.14 28.11 27.28 29.32 30.34 26.28 24.21 20.70 19.09 18.33 24.52 20.75 19.13 20.82 21.86 48.60 498.8 9999.9 4242 39.53 490.0 715.3 440.5 283.3 235.3 6258 9999.9 100.6 53.89 45.00 36.64 32.71 28.07 26.29 25.51 28.00 27.83 22.96 19.55 19.52 17.96 16.33 17.39 23.34 16.24 17.21 18.33 18.93 42.46 492.7 9999.9 4911 500.0 638.0 366.6 271.5 200.0 372.1 9999.9 136.5 56.23 42.05 35.59 29.46 26.16 24.58 22.47 24.66 25.42 21.55 17.68 16.80 16.37 15.31 15.39 15.92 19.73 14.98 15.16 16.23 17.35 42.63 496.7 9999.9 510.0 657.1 365.1 238.3 158.1 148.9 7670 9999.9 61.37 41.72 34.86 28.96 28.86 24.37 23.25 22.87 23.50 20.35 16.21 15.26 13.73 14.42 14.23 13.53 15.82 16.93 13.32 12.48 13.57 16.87 40.87 490.1 520.0 662.9 430.4 221.8 144.6 159.9 428.3 9999.9 112.6 48.37 34.48 29.57 27.37 22.87 20.28 20.74 21.58 18.11 14.48 14.33 13.00 11.97 12.94 13.40 12.43 15.23 12.92 11.42 11.88 12.94 17.15 41.60 530.0 616.9 405.4 219.3 134.2 130.4 133.5 8659 9999.9 57.52 37.00 30.31 24.43 22.55 21.70 20.49 20.94 17.32 13.62 12.30 12.39 10.92 11.82 11.37 11.42 11.89 14.31 11.12 10.85 11.11 13.12 18.43 540.0 622.6 379.5 229.0 118.2 98.04 135.5 423.8 9999.9 122.0 49.99 34.03 26.85 23.67 21.29 20.94 20.07 17.55 14.36 13.03 11.85 10.64 10.58 10.36 10.91 11.14 11.40 12.53 10.06 9.628 11.77 13.69 550.0 480.8 417.7 266.9 123.2 78.07 132.2 92.07 9956 9999.9 60.76 38.93 29.28 24.74 22.30 21.80 19.72 17.97 13.76 12.58 11.21 10.25 9.840 9.802 9.484 10.77 10.11 11.53 10.94 9.544 10.95 11.72 560.0 546.6 357.8 255.7 125.4 85.22 87.69 83.52 462.0 9999.9 114.1 47.09 33.73 25.46 23.71 20.39 19.98 17.88 14.13 12.20 11.68 10.64 9.663 9.647 9.121 9.194 9.511 8.678 11.76 10.28 10.15 11.76 570.0 835.0 439.6 292.6 158.0 103.8 74.06 115.6 112.1 9901 9999.9 65.16 40.73 28.56 23.69 22.21 19.50 16.76 14.64 15.24 12.26 10.37 9.840 8.620 9.098 8.316 8.758 9.529 8.860 11.34 9.120 10.17 580.0 1168 873.4 561.9 394.9 222.6 99.23 146.8 207.0 622.2 9999.9 121.3 48.26 31.23 24.49 20.28 19.38 18.04 14.85 13.74 15.47 11.05 9.234 10.51 9.571 8.367 9.138 8.142 9.235 11.18 9.710 9.516 590.0 4469 1162 963.0 713.2 378.8 158.6 194.7 383.5 436.1 9999.9 9999.9 63.57 40.88 27.25 24.72 21.67 17.21 16.13 12.94 13.54 11.95 10.72 10.30 10.03 9.686 9.478 8.169 8.264 9.883 11.65 11.46 600.0 8530 1404 1343 1044 545.0 192.5 272.9 533.6 630.7 633.4 9999.9 114.7 45.60 32.38 26.19 19.88 19.20 15.93 14.35 11.97 18.92 11.44 10.89 9.457 8.213 8.653 9.347 8.872 8.606 9.024 12.22 610.0 4666 2251 1681 1310 674.7 222.4 314.4 623.8 768.4 296.3 9999.9 9999.9 61.01 38.49 29.38 21.86 17.45 17.59 15.54 14.45 12.21 18.06 10.94 10.40 10.42 9.920 9.873 8.731 8.639 8.838 10.50 620.0 2132 5694 1873 1440 767.3 232.0 340.2 687.5 872.0 306.9 476.3 9999.9 109.3 47.79 33.61 25.09 20.70 18.85 16.98 16.39 12.77 15.09 13.19 11.96 10.53 10.37 9.553 8.559 9.526 8.307 8.519 630.0 2343 9999.9 1873 1379 760.1 250.9 322.3 687.7 837.6 304.9 95.45 9999.9 9999.9 61.43 40.67 28.27 24.90 19.90 18.28 16.85 13.93 12.92 23.59 11.37 10.85 11.93 10.37 9.210 8.809 6.957 7.509 640.0 1869 6373 1940 1414 725.4 254.4 320.7 656.3 790.9 315.7 76.06 465.6 9999.9 113.4 47.98 35.51 26.78 22.09 19.78 16.70 14.86 13.50 12.73 23.92 11.25 11.20 11.35 9.236 8.572 8.073 7.927 650.0 1741 2078 4883 1239 661.8 212.7 312.5 587.8 719.8 275.2 65.87 84.45 9999.9 9999.9 61.77 40.75 31.55 27.53 22.40 19.41 16.89 15.12 13.53 20.62 14.58 11.24 11.45 11.06 8.469 7.410 7.990 660.0 1483 1982 9999.9 1039 652.9 201.5 283.6 497.5 625.7 250.0 75.62 65.98 465.8 9999.9 114.0 46.72 37.25 29.56 25.01 21.00 18.88 16.73 16.33 14.43 33.91 12.38 11.82 10.60 9.634 8.640 7.710 670.0 1807 1569 6931 1244 560.5 193.3 236.4 434.0 545.7 221.9 93.80 61.27 84.67 9999.9 9999.9 60.74 44.10 34.41 27.78 25.20 22.36 20.00 18.93 17.33 16.45 31.16 12.45 10.42 9.792 8.367 8.538 680.0 1313 1433 1525 4957 517.8 184.0 230.7 380.0 476.9 207.3 70.15 68.40 64.69 473.1 9999.9 106.2 51.94 40.17 34.52 26.87 26.02 22.08 20.08 15.85 16.64 32.09 17.33 10.84 11.22 11.78 8.446 690.0 1004 1310 1013 9999.9 443.0 192.9 215.8 345.8 404.5 180.1 67.01 81.29 62.48 91.11 9999.9 9999.9 65.18 44.15 37.21 31.21 27.25 23.12 23.85 21.13 18.75 19.04 62.35 12.11 10.57 9.662 9.110 700.0 1199 935.5 1035 8366 556.1 190.8 204.8 277.2 324.1 166.8 61.93 72.34 55.21 70.17 477.9 9999.9 106.9 54.84 41.14 33.64 30.18 27.39 24.01 21.06 19.27 18.16 20.67 45.55 10.39 9.762 9.651